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Usually Silica aerogels were prepared by hydrolysis and polycondensation of solvent (alcohol) diluted alkoxide in the presence of a catalyst. The hydrolysis and polycondensation reaction mechanism for tetraethoxysilane (TEOS) precursor is as given below: Hydrolysis: Si(OC 2 H 5 )4 + 4 H 2O → Si(OH )4 + 4C 2 H 5OH (1) A catalyst (Critic acid) is used here. Condensation: Si(OH )4 + Si(OH )4 →≡ Si − O − Si ≡ +4 H 2O (2) Si(OH )4 + Si(OC 2 H 5 )4 →≡ Si − O − Si ≡ +4C 2 H 5OH (3) Similarly, tetramethoxysilane (TMOS) and polyethoxydisiloxane (PEDS) precursors follow the same trend of chemical reactions.

M. ; Gonçalves, H. M. ; Mendonça, C. & Esteves da Silva, J. C. G. (2008). Multiway chemometric decomposition of EEM of fluorescence of CdTe quantum dots obtained as function of pH. ; Shih, W. Y. & Shih, W. H. (2007). Non-heavy-metal ZnS quantum dots with bright blue photoluminescence by a one-step aqueous synthesis. Nanotechnology, 18, 205604-205609, ISSN: 0957-4484 Ling J. & Cong R. M. (2008). Fabrication of photoluminescent ultra-thin film by using CdSZnS core-shell structure quantum dot/PAMAM dendrimer nanocomposites.

Peptide-coated CdS quantum dots for the optical detection of copper(II) and silver(I). Chemical Communications, 21, 26842685, ISSN: 1364-548X Gayen, S. ; Das, B. ; Liang, X. ; Alfano, R. ; Byro, A. ; Bauer, D. L. V. & Balogh-Nair, V. (2007). Synthesis and optical spectroscopy of a hybrid cadmium sulphide dendrimer nanocomposite. Journal Optical Society of America B, 24, 3064-3071, ISSN: 0740-3224 Gonçalves, H. M. ; Mendonça, C. & Esteves da Silva, J. C. G. (2009). PARAFAC Analysis of the Quenching of EEM of Fluorescence of Glutathione Capped CdTe Quantum Dots by Pb(II).

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